5BVS

Linoleate-bound pFABP4

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron site	PAL/PLS
Beamline	7A (6B, 6C1)
Temperature [K]	100
Detector technology	CCD
Collection date	2015-02-25
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9794
Spacegroup name	P 61
Unit cell lengths	60.487, 60.487, 139.569
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	29.560 - 2.200
R-factor	0.18885
Rwork	0.187
R-free	0.22606
RMSD bond length	0.029
RMSD bond angle	2.525
Refinement software	REFMAC (5.8.0049)

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000
High resolution limit [Å]	2.200
Number of reflections	28819
<I/σ(I)>	55.9
Completeness [%]	99.7
Redundancy	10.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.1 M CHES (pH 9.5), 30% (w/v) PEG 3000