5BVS
Linoleate-bound pFABP4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-02-25 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9794 |
Spacegroup name | P 61 |
Unit cell lengths | 60.487, 60.487, 139.569 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.560 - 2.200 |
R-factor | 0.18885 |
Rwork | 0.187 |
R-free | 0.22606 |
RMSD bond length | 0.029 |
RMSD bond angle | 2.525 |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.200 |
Number of reflections | 28819 |
<I/σ(I)> | 55.9 |
Completeness [%] | 99.7 |
Redundancy | 10.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M CHES (pH 9.5), 30% (w/v) PEG 3000 |