5BR6
Crystal structure of hemagglutinin of A/Taiwan/2/2013 (H6N1) in complex with LSTc
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-G |
| Synchrotron site | APS |
| Beamline | 21-ID-G |
| Temperature [K] | 80 |
| Detector technology | CCD |
| Collection date | 2014-10-24 |
| Detector | RAYONIX MX-300 |
| Wavelength(s) | 0.978 |
| Spacegroup name | P 3 |
| Unit cell lengths | 113.670, 113.670, 163.160 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 37.683 - 2.430 |
| R-factor | 0.204 |
| Rwork | 0.203 |
| R-free | 0.22490 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHENIX |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 37.690 |
| High resolution limit [Å] | 2.430 |
| Number of reflections | 88853 |
| <I/σ(I)> | 9.7 |
| Completeness [%] | 100.0 |
| Redundancy | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 9 | 290 | 0.1 M Bicine, pH 9.0, 10% PEG 20000 and 2% 1,4-Dioxane |
