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5BPB

Crystal structure of the cysteine-rich domain of human Frizzled 4 - Crystal Form I

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I24
Synchrotron siteDiamond
BeamlineI24
Temperature [K]100
Detector technologyPIXEL
Collection date2013-02-17
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.9686
Spacegroup nameP 21 21 21
Unit cell lengths72.608, 102.140, 116.508
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution40.000 - 2.200
R-factor0.179
Rwork0.177
R-free0.22270
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1ijy
RMSD bond length0.007
RMSD bond angle1.279
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwareREFMAC (5.7.0032)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]41.7702.270
High resolution limit [Å]2.2002.200
Rmerge0.0770.911
Number of reflections44268
<I/σ(I)>12.82
Completeness [%]99.299.7
Redundancy4.34.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.52941.6 M tri-sodium citrate, pH 6.5

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