5BP5
Crystal structure of HA17-HA33-IPT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-03-21 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979180 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 105.868, 118.928, 162.197 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.950 - 2.180 |
R-factor | 0.2274 |
Rwork | 0.227 |
R-free | 0.23850 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 47.950 |
High resolution limit [Å] | 2.180 |
Number of reflections | 53512 |
<I/σ(I)> | 15.1 |
Completeness [%] | 99.5 |
Redundancy | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.1 M MES, 0.1 M magnesium chloride, 5% PEG 8000 |