5BNY
Crystal structure of hemagglutinin of A/Chicken/Guangdong/S1311/2010 (H6N6)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-G |
Synchrotron site | APS |
Beamline | 21-ID-G |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2014-10-24 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.978 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 69.260, 137.370, 198.870 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.750 - 2.660 |
R-factor | 0.2042 |
Rwork | 0.202 |
R-free | 0.24510 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ruz |
RMSD bond length | 0.004 |
RMSD bond angle | 0.907 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.690 | 2.800 |
High resolution limit [Å] | 2.660 | 2.660 |
Rmerge | 0.104 | 0.487 |
Number of reflections | 53602 | |
<I/σ(I)> | 12.4 | 2.7 |
Completeness [%] | 96.9 | 89.7 |
Redundancy | 4.4 | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 290 | 0.1 M Bis-Tris propane, 2.3 M (NH4)2SO4 |