5BND
Crystal structure of the C-terminal domain of TagH
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13C1 |
Synchrotron site | NSRRC |
Beamline | BL13C1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-03-06 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 104.576, 124.749, 56.132 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.413 - 2.680 |
R-factor | 0.2085 |
Rwork | 0.206 |
R-free | 0.25740 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.320 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 33.413 |
High resolution limit [Å] | 2.680 |
Number of reflections | 18143 |
<I/σ(I)> | 3 |
Completeness [%] | 99.2 |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | 12 % PEG 3350, 0.1 M malic acid (pH 7.0). |