5B79
Crystal structure of DPF2 double PHD finger
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-02-05 |
Detector | DECTRIS PILATUS 200K |
Wavelength(s) | 1.5418 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 106.979, 106.979, 52.592 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.599 - 2.601 |
R-factor | 0.1941 |
Rwork | 0.189 |
R-free | 0.23800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4llb |
RMSD bond length | 0.006 |
RMSD bond angle | 0.940 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 23.600 | 2.640 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 4902 | |
<I/σ(I)> | 29.9 | |
Completeness [%] | 99.6 | |
Redundancy | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | ammonium citrate tribasic, Bis-Tris propane |