5B4M
Crystal structure of an Fab against human influenza A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | OXFORD DIFFRACTION ENHANCE ULTRA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-07-07 |
Detector | OXFORD RUBY CCD |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 51.592, 90.940, 81.442 |
Unit cell angles | 90.00, 92.21, 90.00 |
Refinement procedure
Resolution | 81.380 - 2.400 |
R-factor | 0.28785 |
Rwork | 0.285 |
R-free | 0.33796 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.561 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 81.380 | 2.440 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.070 | 0.445 |
Number of reflections | 27507 | |
<I/σ(I)> | 16.1 | 2.2 |
Completeness [%] | 98.5 | 97.7 |
Redundancy | 3.5 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 294 | PEG 3350, NaCl, Bis-Tris |