5B4H
Crystal structure of I86D mutant of phycocyanobilin:ferredoxin oxidoreductase in complex with biliverdin (data 1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-02-04 |
Detector | RIGAKU JUPITER 210 |
Wavelength(s) | 0.9000 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 70.833, 95.691, 42.398 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.110 |
Rwork | 0.122 |
R-free | 0.15590 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 4qcd |
RMSD bond length | 0.016 |
RMSD bond angle | 0.032 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.900 | 1.150 |
High resolution limit [Å] | 1.100 | 1.100 |
Rmerge | 0.370 | |
Number of reflections | 113410 | |
<I/σ(I)> | 14.2 | |
Completeness [%] | 99.1 | 100 |
Redundancy | 14.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | sodium citrate, sodium chloride, Tris |