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5B49

Crystal structure of LpxH with manganese from Pseudomonas aeruginosa

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL41XU
Synchrotron siteSPring-8
BeamlineBL41XU
Temperature [K]100
Detector technologyCCD
Collection date2011-02-17
DetectorRAYONIX MX225HE
Wavelength(s)1.0000, 1.8925
Spacegroup nameP 1 21 1
Unit cell lengths48.937, 108.862, 51.555
Unit cell angles90.00, 92.68, 90.00
Refinement procedure
Resolution29.230 - 1.650
R-factor0.15288
Rwork0.152
R-free0.17662
Structure solution methodMAD
RMSD bond length0.011
RMSD bond angle1.403
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareSHELXCD
Refinement softwareREFMAC (5.8.0135)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.710
High resolution limit [Å]1.6501.650
Number of reflections64565
<I/σ(I)>20.42.23
Completeness [%]100.0100
Redundancy6.76.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.62930.2M L-Proline, 0.1M HEPES pH 7.6, 8.5% PEG 3350

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