5B1R
Crystal structure of mouse CD72a CTLD
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-17A |
| Synchrotron site | Photon Factory |
| Beamline | BL-17A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-05-23 |
| Detector | ADSC QUANTUM 270 |
| Wavelength(s) | 0.9800 |
| Spacegroup name | P 61 |
| Unit cell lengths | 65.472, 65.472, 61.220 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 26.936 - 1.200 |
| R-factor | 0.1294 |
| Rwork | 0.128 |
| R-free | 0.14790 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1fm5 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.206 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.220 |
| High resolution limit [Å] | 1.200 | 1.200 |
| Rmerge | 0.794 | |
| Number of reflections | 46533 | |
| <I/σ(I)> | 42.8 | 4.1 |
| Completeness [%] | 99.8 | 100 |
| Redundancy | 11 | 10.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | imidazole, sodium acetate trihydrate, hexamine cobalt (III) chloride |
