5B1G
Crystal structure of hen egg-white lysozyme
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | FREE ELECTRON LASER |
Source details | SACLA BEAMLINE BL3 |
Synchrotron site | SACLA |
Beamline | BL3 |
Temperature [K] | 300 |
Detector technology | CCD |
Collection date | 2014-11-25 |
Detector | MPCCD |
Wavelength(s) | 1.77 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 80.300, 80.300, 38.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.390 - 2.300 |
R-factor | 0.1825 |
Rwork | 0.181 |
R-free | 0.21060 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3wul |
RMSD bond length | 0.009 |
RMSD bond angle | 1.162 |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.340 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 5983 | |
<I/σ(I)> | 9.8 | 7.6 |
Completeness [%] | 100.0 | 100 |
Redundancy | 502 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 293 | NaCl |