5B0O
Structure of the FliH-FliI complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 40 |
Detector technology | CCD |
Collection date | 2010-02-03 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 133.662, 147.305, 164.233 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 51.315 - 3.000 |
R-factor | 0.2203 |
Rwork | 0.218 |
R-free | 0.27030 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2dpy |
RMSD bond length | 0.005 |
RMSD bond angle | 0.998 |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX (1.7.1_743) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.000 | 3.160 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.109 | 0.362 |
Number of reflections | 65054 | |
<I/σ(I)> | 9.4 | 3.5 |
Completeness [%] | 99.4 | 99.6 |
Redundancy | 4.6 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.2 | 285 | 5%(w/v) PEG400, 0.1M HEPES pH7.2 and 100mM Magnesium acetate |