5B05
Lysozyme (control experiment)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2015-05-09 |
Detector | RIGAKU RAXIS VII |
Wavelength(s) | 1.54 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.816, 78.816, 36.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.730 - 1.800 |
R-factor | 0.15203 |
Rwork | 0.150 |
R-free | 0.18733 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2yvb |
RMSD bond length | 0.020 |
RMSD bond angle | 1.759 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 100.000 |
High resolution limit [Å] | 1.800 |
Number of reflections | 11259 |
<I/σ(I)> | 44.8 |
Completeness [%] | 100.0 |
Redundancy | 13.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | NaCl, Ethylene glycol |