5AZU
CRYSTAL STRUCTURE ANALYSIS OF OXIDIZED PSEUDOMONAS AERUGINOSA AZURIN AT PH 5.5 AND PH 9.0. A PH-INDUCED CONFORMATIONAL TRANSITION INVOLVES A PEPTIDE BOND FLIP
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 57.760, 81.090, 109.940 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 * - 1.930* |
R-factor | 0.175 * |
RMSD bond length | 0.011 |
RMSD bond angle | 2.700 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 9999.000 * |
High resolution limit [Å] | 1.930 * |
Rmerge | 0.096 * |
Total number of observations | 135274 * |
Number of reflections | 34125 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 13 (mg/ml) | |
2 | 1 | drop | ammonium sulphate | 1.5 (M) | |
3 | 1 | drop | lithium nitrate | 0.4 (M) | |
4 | 1 | drop | acetate | 0.1 (M) | |
5 | 1 | reservoir | ammonium sulphate | 4.0 (M) | |
6 | 1 | reservoir | lithium nitrate | 0.7 (M) | |
7 | 1 | reservoir | acetate | 0.1 (M) |