5AXU
Crystal Structure of Cypovirus Polyhedra R13A Mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL32XU |
Synchrotron site | SPring-8 |
Beamline | BL32XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-07-19 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 1.0 |
Spacegroup name | I 2 3 |
Unit cell lengths | 103.229, 103.229, 103.229 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.640 - 1.600 |
R-factor | 0.162 |
Rwork | 0.160 |
R-free | 0.18900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2oh6 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.356 |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 24339 | |
<I/σ(I)> | 14.2 | 2.5 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5 | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | IN CELL | 7 | 300 | IN VIVO CRYSTALLIZATION IN THE CYTOPLASM OF THE CELL, PH 7.0, TEMPERATURE 300K |