5AUZ
Crystal structure of DAPK1 in complex with genistein.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-05-18 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.720, 62.318, 88.640 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.400 - 1.600 |
R-factor | 0.1783 |
Rwork | 0.177 |
R-free | 0.20580 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.074 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 34.400 |
High resolution limit [Å] | 1.600 |
Number of reflections | 34651 |
<I/σ(I)> | 21 |
Completeness [%] | 98.9 |
Redundancy | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 2 M ammonium sulfate, 0.1 M MES |