5AUX

Crystal structure of DAPK1 in complex with kaempferol.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NW12A
Synchrotron site	Photon Factory
Beamline	AR-NW12A
Temperature [K]	100
Detector technology	CCD
Collection date	2014-06-14
Detector	ADSC QUANTUM 210r
Wavelength(s)	1
Spacegroup name	P 21 21 21
Unit cell lengths	46.823, 62.193, 88.440
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	37.400 - 1.500
R-factor	0.1795
Rwork	0.178
R-free	0.20770
RMSD bond length	0.007
RMSD bond angle	1.153
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	PHENIX
Refinement software	PHENIX ((phenix.refine: 1.8_1069))

Data quality characteristics

	Overall
Low resolution limit [Å]	37.400
High resolution limit [Å]	1.500
Number of reflections	41548
<I/σ(I)>	27.2
Completeness [%]	98.6
Redundancy	5.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	2 M ammonium sulfate, 0.1 M MES