5AUT
Crystal structure of DAPK1 in complex with ANS.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-04-18 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.774, 62.260, 88.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.453 - 1.700 |
R-factor | 0.1719 |
Rwork | 0.170 |
R-free | 0.20240 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1jks |
RMSD bond length | 0.007 |
RMSD bond angle | 1.127 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 44.300 |
High resolution limit [Å] | 1.700 |
Number of reflections | 28573 |
<I/σ(I)> | 31.6 |
Completeness [%] | 97.6 |
Redundancy | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 2 M ammonium sulfate, 0.1 M MES |