5APE
Hen Egg White Lysozyme reference dataset odd frames
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 297 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 2M-F |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.240, 79.240, 37.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.090 - 1.700 |
R-factor | 0.16998 |
Rwork | 0.169 |
R-free | 0.19217 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.017 |
RMSD bond angle | 1.667 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 1.740 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.080 | 0.570 |
Number of reflections | 12140 | |
<I/σ(I)> | 84.49 | 12.95 |
Completeness [%] | 93.4 | 13 |
Redundancy | 182 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.5 | 30-100MG/ML HEWL IN 50MM NAAC PH 4.5 RESERVOIR: 50MM NAAC PH 4.5 1M NACL 25% ETHYLENE GLYCOL |