5AO5
Endo180 D1-4, monoclinic form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-10-05 |
Detector | DECTRIS PIXEL |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 126.370, 92.370, 127.650 |
Unit cell angles | 90.00, 100.31, 90.00 |
Refinement procedure
Resolution | 60.158 - 2.480 |
R-factor | 0.1961 |
Rwork | 0.194 |
R-free | 0.24420 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 1TDQ 3m7p 1dqg |
RMSD bond length | 0.006 |
RMSD bond angle | 0.901 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 62.800 | 2.540 |
High resolution limit [Å] | 2.480 | 2.480 |
Rmerge | 0.050 | 0.480 |
Number of reflections | 50153 | |
<I/σ(I)> | 15.4 | 2.2 |
Completeness [%] | 97.8 | 98.4 |
Redundancy | 3.3 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | pH 7.5 |