5AMZ
Crystal Structure of Thaumatin processed with the CrystalDirect automated mounting and cryo-cooling technology
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 57.515, 57.515, 150.237 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.400 |
R-factor | 0.18052 |
Rwork | 0.179 |
R-free | 0.20332 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.024 |
RMSD bond angle | 2.237 |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.400 |
Rmerge | 0.100 |
Number of reflections | 50733 |
Completeness [%] | 100.0 |
Redundancy | 10.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |