5AHX
Apo structure of soluble epoxide hydrolase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | RIGAKU SATURN A200 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 91.738, 91.738, 245.273 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 79.450 - 2.000 |
Rwork | 0.171 |
R-free | 0.21850 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.130 |
Data reduction software | XDS |
Data scaling software | SCALA |
Refinement software | BUSTER (2.9.5) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 245.000 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.180 | 0.880 |
Number of reflections | 42307 | |
<I/σ(I)> | 15 | 3.2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 12.7 | 12.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |