5AFM

alpha7-AChBP in complex with lobeline and fragment 4

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	100
Detector technology	CCD
Collection date	2013-11-30
Detector	ADSC CCD
Spacegroup name	P 21 21 21
Unit cell lengths	75.700, 119.600, 143.300
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.720 - 2.850
R-factor	0.1642
Rwork	0.161
R-free	0.21720
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.010
RMSD bond angle	1.280
Refinement software	BUSTER (2.8.0)

Data quality characteristics

	Overall
Low resolution limit [Å]	47.780
High resolution limit [Å]	2.780
Rmerge	0.090
Number of reflections	33519
<I/σ(I)>	11
Completeness [%]	99.9
Redundancy	4.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1