5AFL

alpha7-AChBP in complex with lobeline and fragment 3

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	100
Collection date	2013-04-02
Spacegroup name	P 21 21 21
Unit cell lengths	85.808, 112.300, 143.720
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	41.829 - 2.385
R-factor	0.1738
Rwork	0.171
R-free	0.23100
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.007
RMSD bond angle	1.123
Refinement software	PHENIX ((PHENIX.REFINE: 1.8_1069))

Data quality characteristics

	Overall
Low resolution limit [Å]	47.910
High resolution limit [Å]	2.350
Rmerge	0.080
Number of reflections	58398
<I/σ(I)>	15.8
Completeness [%]	99.8
Redundancy	5.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1