5AFH

alpha7-AChBP in complex with lobeline

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	100
Detector technology	CCD
Collection date	2014-05-21
Detector	ADSC CCD
Spacegroup name	P 21 21 21
Unit cell lengths	85.520, 112.504, 143.109
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	44.223 - 2.400
R-factor	0.1709
Rwork	0.168
R-free	0.22720
Structure solution method	OTHER
RMSD bond length	0.009
RMSD bond angle	1.229
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	48.590
High resolution limit [Å]	2.700
Rmerge	0.070
Number of reflections	38863
<I/σ(I)>	16.7
Completeness [%]	99.6
Redundancy	4.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1