5AF3
X-RAY CRYSTAL STRUCTURE OF RV2018 FROM MYCOBACTERIUM TUBERCULOSIS
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE BW7A |
| Synchrotron site | BESSY |
| Beamline | BW7A |
| Temperature [K] | 100 |
| Spacegroup name | P 31 |
| Unit cell lengths | 81.935, 81.935, 75.361 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 70.890 - 1.780 |
| R-factor | 0.21264 |
| Rwork | 0.210 |
| R-free | 0.25421 |
| Structure solution method | SIRAS |
| Starting model (for MR) | NONE |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.960 | 1.870 |
| High resolution limit [Å] | 1.770 | 1.770 |
| Rmerge | 0.050 | 0.460 |
| Number of reflections | 53660 | |
| <I/σ(I)> | 10.73 | |
| Completeness [%] | 97.5 | 83.5 |
| Redundancy | 3.81 | 3.55 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
