Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-2 |
| Synchrotron site | ESRF |
| Beamline | ID23-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-11-28 |
| Detector | ADSC CCD |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 73.861, 72.329, 73.528 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 52.110 - 2.840 |
| R-factor | 0.2378 |
| Rwork | 0.236 |
| R-free | 0.27260 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3bev |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.830 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.10.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 73.780 | 2.990 |
| High resolution limit [Å] | 2.840 | 2.840 |
| Rmerge | 0.160 | 0.410 |
| Number of reflections | 9390 | |
| <I/σ(I)> | 11 | 2 |
| Completeness [%] | 96.5 | 87.7 |
| Redundancy | 5.8 | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8 | 0.2M MAGNESIUM CHLORIDE HEXAHYDRATE, 0.1M TRIS, PH 8.0, 20% PEG 6000 |
