5ACF
X-ray Structure of LPMO
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-3 |
Synchrotron site | MAX II |
Beamline | I911-3 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 124.710, 124.710, 124.710 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.800 |
R-factor | 0.17279 |
Rwork | 0.171 |
R-free | 0.21249 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4eir |
RMSD bond length | 0.016 |
RMSD bond angle | 1.761 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.850 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.160 | 0.910 |
Number of reflections | 25307 | |
<I/σ(I)> | 7.27 | 1.38 |
Completeness [%] | 81.1 | 80.5 |
Redundancy | 2.63 | 2.68 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 3.6M SODIUM CHLORIDE, 100MM CITRIC ACID PH4.0 (PH5.5) |