5A9W
Structure of GDPCP BipA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-07-17 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | I 41 3 2 |
| Unit cell lengths | 237.554, 237.554, 237.554 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.490 - 3.700 |
| R-factor | 0.24869 |
| Rwork | 0.244 |
| R-free | 0.30863 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3e3x |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.690 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0107) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.490 | 3.860 |
| High resolution limit [Å] | 3.660 | 3.660 |
| Rmerge | 0.140 | 1.450 |
| Number of reflections | 12870 | |
| <I/σ(I)> | 14.3 | 2.1 |
| Completeness [%] | 99.5 | 97.2 |
| Redundancy | 18.7 | 17.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
