5A9P

Crystal structure of Operophtera brumata CPV18 polyhedra

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I24
Synchrotron site	Diamond
Beamline	I24
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS 6M
Spacegroup name	I 2 3
Unit cell lengths	102.770, 102.770, 102.770
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	72.669 - 1.476
R-factor	0.1311
Rwork	0.130
R-free	0.14750
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2oh6
RMSD bond length	0.005
RMSD bond angle	1.146
Data reduction software	xia2
Data scaling software	xia2
Phasing software	PHASER
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	72.700	1.510
High resolution limit [Å]	1.480	1.480
Rmerge	0.320
Number of reflections	30415
<I/σ(I)>	7.1	1.5
Completeness [%]	100.0	99.8
Redundancy	12.9	8.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7.5		PH 7.5