5A9B

Crystal structure of Bombyx mori CPV1 polyhedra base domain deleted mutant

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I24
Synchrotron site	Diamond
Beamline	I24
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS 6M
Spacegroup name	I 2 3
Unit cell lengths	103.860, 103.860, 103.860
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.401 - 1.883
R-factor	0.1916
Rwork	0.189
R-free	0.25110
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2oh6
RMSD bond length	0.003
RMSD bond angle	0.790
Data reduction software	xia2
Data scaling software	xia2
Phasing software	PHASER
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.400	1.930
High resolution limit [Å]	1.880	1.880
Rmerge	0.230
Number of reflections	15023
<I/σ(I)>	4.8	1
Completeness [%]	98.8	98.6
Redundancy	4.3	4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7.5		pH 7.5