5A99
Crystal structure of Operophtera brumata CPV19 polyhedra
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 102.720, 102.720, 102.720 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 41.935 - 1.511 |
| R-factor | 0.1693 |
| Rwork | 0.166 |
| R-free | 0.22810 |
| Structure solution method | SIRAS |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.124 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | SHARP |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 51.400 | 1.590 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Rmerge | 0.370 | |
| Number of reflections | 21653 | |
| <I/σ(I)> | 3.8 | 0.3 |
| Completeness [%] | 75.5 | 12.2 |
| Redundancy | 3.8 | 1.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | pH 7.5 |
