5A8S
Crystal structure of Antheraea mylitta CPV4 polyhedra type 1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MARRESEARCH |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 101.682, 101.682, 101.682 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 29.353 - 1.724 |
| R-factor | 0.123 |
| Rwork | 0.118 |
| R-free | 0.16580 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2OH6 AND STRUCTURE OF CPV5 POLYHEDRIN |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.092 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHASER |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.400 | 1.820 |
| High resolution limit [Å] | 1.720 | 1.720 |
| Rmerge | 0.200 | 0.380 |
| Number of reflections | 17233 | |
| <I/σ(I)> | 9.7 | 1.7 |
| Completeness [%] | 92.7 | 59 |
| Redundancy | 11.4 | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | pH 7.5 |
