5A8S

Crystal structure of Antheraea mylitta CPV4 polyhedra type 1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I24
Synchrotron site	Diamond
Beamline	I24
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	I 2 3
Unit cell lengths	101.682, 101.682, 101.682
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.353 - 1.724
R-factor	0.123
Rwork	0.118
R-free	0.16580
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2OH6 AND STRUCTURE OF CPV5 POLYHEDRIN
RMSD bond length	0.006
RMSD bond angle	1.092
Data reduction software	xia2
Data scaling software	xia2
Phasing software	PHASER
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	29.400	1.820
High resolution limit [Å]	1.720	1.720
Rmerge	0.200	0.380
Number of reflections	17233
<I/σ(I)>	9.7	1.7
Completeness [%]	92.7	59
Redundancy	11.4	1.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7.5		pH 7.5