5A7Q
Crystal structure of human JMJD2A in complex with compound 30
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-03-06 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 101.194, 149.080, 57.627 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 83.727 - 2.000 |
Rwork | 0.194 |
R-free | 0.23140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2oq7 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 149.080 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.050 | 0.610 |
Number of reflections | 59779 | |
<I/σ(I)> | 19.2 | 2.3 |
Completeness [%] | 99.9 | 99.8 |
Redundancy | 5.4 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 28% PEG3350 -- 0.1M BIS-TRIS PH 6.5 -- 0.15M AMMONIUM SULFATE |