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5A6W

Complex of rice blast (Magnaporthe oryzae) effector protein AVR-PikD with the HMA domain of Pikp1 from rice (Oryza sativa)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Temperature [K]100
Detector technologyPIXEL
Collection date2014-07-10
DetectorDECTRIS PILATUS 6M
Spacegroup nameP 41 21 2
Unit cell lengths118.410, 118.410, 35.810
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution39.470 - 1.600
R-factor0.17908
Rwork0.178
R-free0.20544
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)5a6p
RMSD bond length0.013
RMSD bond angle1.567
Data reduction softwarexia2
Data scaling softwarexia2
Refinement softwareREFMAC (5.8.0073)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]39.4701.640
High resolution limit [Å]1.6001.600
Rmerge0.0500.650
Number of reflections32549
<I/σ(I)>32.34.7
Completeness [%]100.0100
Redundancy17.717.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
12M AMMONIUM SULPHATE, 0.1M CHES PH 9 AND 20% PEG335

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