5A5Y
Crystal structure of AtTTM3 in complex with tripolyphosphate and magnesium ion (form A)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-02-17 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | I 4 2 2 |
| Unit cell lengths | 136.334, 136.334, 144.202 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 45.370 - 1.920 |
| R-factor | 0.15734 |
| Rwork | 0.153 |
| R-free | 0.19827 |
| Structure solution method | SIRAS |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.268 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | SHELXD |
| Refinement software | REFMAC (5.8.0123) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.330 | 2.040 |
| High resolution limit [Å] | 1.920 | 1.920 |
| Rmerge | 0.080 | 1.210 |
| Number of reflections | 49737 | |
| <I/σ(I)> | 20.06 | 2.18 |
| Completeness [%] | 98.5 | 90.8 |
| Redundancy | 10.59 | 8.35 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5 | 2.2 M NACL, 0.1 M CITRIC ACID/NAOH PH 5.0 |
