5A4H
Solution structure of the lipid droplet anchoring peptide of CGI-58 bound to DPC micelles
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | DD2 | 600 | |
| 2 | Varian | 700 | ||
| 3 | Bruker | 750 | ||
| 4 | Varian | 500 | ||
| 5 | Bruker | 900 | ||
| 6 | Bruker | 900 | ||
| 7 | Bruker | 900 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | HNCA |
| 10 | 5 | 1 | TOCSY_90MS |
| 11 | 6 | 1 | 13CHSQC_B900 |
| 12 | 6 | 1 | CNOESY_B900 |
| 13 | 7 | 1 | NOESY_200MS |
| 2 | 1 | 1 | HNCACB |
| 3 | 1 | 1 | HNCACO |
| 4 | 1 | 1 | HSQC |
| 5 | 2 | 1 | HSQC_ANOESY |
| 6 | 2 | 1 | NOESYHSQC |
| 7 | 3 | 1 | HCCONH |
| 8 | 4 | 1 | CCONH |
| 9 | 4 | 1 | HCCH_TOCSY |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6 | 1.0 | 310 |
| 2 | 6 | 1.0 | 310 |
| 3 | 6 | 1.0 | 310 |
| 4 | 6 | 1.0 | 310 |
| 5 | 6 | 1.0 | 303 |
| 6 | 6 | 1.0 | 310 |
| 7 | 6 | 1.0 | 303 |
Conformers
| Conformers Calculated Total Number | 100 |
| Conformers Submitted Total Number | 20 |
