5A47

Structure of Thaumatin obtained by multi crystal data collection

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID23-1
Synchrotron site	ESRF
Beamline	ID23-1
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS 6M
Spacegroup name	P 41 21 2
Unit cell lengths	57.927, 57.927, 150.642
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 1.200
R-factor	0.13383
Rwork	0.133
R-free	0.15128
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.028
RMSD bond angle	2.178
Refinement software	REFMAC (5.8.0103)

Data quality characteristics

	Overall
Low resolution limit [Å]	19.760
High resolution limit [Å]	1.190
Rmerge	0.090
Number of reflections	81704
Completeness [%]	99.4
Redundancy	51.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1