5A3D
Structural insights into the recognition of cisplatin and AAF-dG lesions by Rad14 (XPA)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 41 |
Unit cell lengths | 53.727, 53.727, 130.551 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 53.730 - 1.800 |
R-factor | 0.21109 |
Rwork | 0.210 |
R-free | 0.24076 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.018 |
RMSD bond angle | 2.154 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 65.300 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.080 | 0.890 |
Number of reflections | 34232 | |
<I/σ(I)> | 10.7 | 2.6 |
Completeness [%] | 99.8 | 95.6 |
Redundancy | 7.4 | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.18 M AMMONIUM NITRATE AND 40% 2-METHYL- 1,3,-PROPANEDIOL |