5A39
Structure of Rad14 in complex with cisplatin containing DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-07-30 |
Detector | ADSC CCD |
Spacegroup name | P 41 |
Unit cell lengths | 54.421, 54.421, 130.773 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.420 - 2.800 |
R-factor | 0.21462 |
Rwork | 0.213 |
R-free | 0.25554 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | NONE |
RMSD bond length | 0.012 |
RMSD bond angle | 1.570 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.400 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.150 | 1.330 |
Number of reflections | 9402 | |
<I/σ(I)> | 9.1 | 1.2 |
Completeness [%] | 99.7 | 98.1 |
Redundancy | 4.2 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.2M MAGNESIUM ACETATE 0.1M MES PH 6.5 30% MPD |