5A2Z
Crystal structure of mtPAP in complex with GTP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.3 |
| Synchrotron site | BESSY |
| Beamline | 14.3 |
| Temperature [K] | 287 |
| Detector technology | CCD |
| Detector | RAYONIX MX-225 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 59.746, 94.364, 192.014 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 39.670 - 2.450 |
| R-factor | 0.2616 |
| Rwork | 0.260 |
| R-free | 0.29502 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.947 |
| Data reduction software | XDS |
| Data scaling software | SCALEPACK |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | 2.580 |
| High resolution limit [Å] | 2.450 | 2.450 |
| Rmerge | 0.120 | 0.920 |
| Number of reflections | 40389 | |
| <I/σ(I)> | 11.6 | 2.1 |
| Completeness [%] | 99.0 | 98 |
| Redundancy | 7.3 | 7.6 |
| CC(1/2) | 0.990 | 0.520 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
