5A2X
Crystal structure of mtPAP in complex with CTP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.3 |
Synchrotron site | BESSY |
Beamline | 14.3 |
Temperature [K] | 287 |
Detector technology | CCD |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 61.064, 95.575, 191.613 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.290 - 3.100 |
R-factor | 0.21462 |
Rwork | 0.212 |
R-free | 0.25965 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.049 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 3.270 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.160 | 1.160 |
Number of reflections | 21101 | |
<I/σ(I)> | 11.3 | 1.4 |
Completeness [%] | 99.9 | 100 |
Redundancy | 8.2 | 6 |
CC(1/2) | 0.990 | 0.520 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |