5A2P
THE COMPLEX STRUCTURE OF PDZ DOMAINS IN SYNTENIN-1 WITH 4L PEPTIDE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 6C1 |
Synchrotron site | PAL/PLS |
Beamline | 6C1 |
Temperature [K] | 93 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 43 |
Unit cell lengths | 64.200, 64.200, 201.767 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.903 - 2.496 |
R-factor | 0.221 |
Rwork | 0.219 |
R-free | 0.24440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | NONE |
RMSD bond length | 0.003 |
RMSD bond angle | 0.814 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.090 | 0.380 |
Number of reflections | 28305 | |
<I/σ(I)> | 13.96 | 2.57 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5.5 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |