5A1S
Crystal structure of the sodium-dependent citrate symporter SeCitS form Salmonella enterica.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-04-11 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 1 |
| Unit cell lengths | 86.382, 89.935, 91.843 |
| Unit cell angles | 90.44, 113.79, 99.55 |
Refinement procedure
| Resolution | 47.977 - 2.500 |
| R-factor | 0.2099 |
| Rwork | 0.208 |
| R-free | 0.24600 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.762 |
| Data scaling software | Aimless |
| Phasing software | SHELXD |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.600 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Rmerge | 0.050 | 0.870 |
| Number of reflections | 84908 | |
| <I/σ(I)> | 8.9 | 1.3 |
| Completeness [%] | 98.8 | 98.1 |
| Redundancy | 8.2 | 8.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | pH 6.5 |
