Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2011-12-18 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 60.420, 66.890, 67.300 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 33.650 - 1.600 |
| R-factor | 0.2666 |
| Rwork | 0.264 |
| R-free | 0.31242 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2chu |
| RMSD bond length | 0.020 |
| RMSD bond angle | 2.370 |
| Data reduction software | xia2 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.960 | 1.650 |
| High resolution limit [Å] | 1.610 | 1.610 |
| Rmerge | 0.050 | 0.420 |
| Number of reflections | 204289 | |
| <I/σ(I)> | 18.3 | 2.2 |
| Completeness [%] | 99.5 | 94.9 |
| Redundancy | 5.7 | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | 0.2M SODIUM NITRATE, 0.1M BIS TRIS PROPANE PH 7.5, 20% PEG 3350 |
