5ZWY
Ribokinase from Leishmania donovani
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | RRCAT INDUS-2 BEAMLINE PX-BL21 |
Synchrotron site | RRCAT INDUS-2 |
Beamline | PX-BL21 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-08-18 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.9794 |
Spacegroup name | P 61 |
Unit cell lengths | 100.253, 100.253, 126.771 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.610 - 1.950 |
R-factor | 0.18438 |
Rwork | 0.183 |
R-free | 0.21781 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2fv7 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.340 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0230) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.610 | 2.000 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.101 | 0.604 |
Number of reflections | 52575 | 27813 |
<I/σ(I)> | 0.101 | |
Completeness [%] | 100.0 | |
Redundancy | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.3 | 296 | Citric acid, NaCl, Glycerol |