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5ZC5

uPA-NU-09F

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNFPSS BEAMLINE BL19U1
Synchrotron siteNFPSS
BeamlineBL19U1
Temperature [K]100
Detector technologyPIXEL
Collection date2015-03-29
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.979
Spacegroup nameH 3
Unit cell lengths120.698, 120.698, 42.769
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution60.000 - 1.900
R-factor0.205
Rwork0.203
R-free0.23500
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4dve
RMSD bond length0.007
RMSD bond angle1.432
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareREFMAC (5.8.0103)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]60.0001.930
High resolution limit [Å]1.9001.900
Rmerge0.1140.796
Number of reflections18272
<I/σ(I)>22
Completeness [%]99.8
Redundancy5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP29850mM sodium citrate pH 4.6, 1.95M (NH4)2SO4, 0.03% NaN3, 5% PEG 400

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