5YV1
DNA polymerase IV - DNA ternary complex 13
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-09-18 |
Detector | MAR CCD 130 mm |
Wavelength(s) | 0.95372 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 86.070, 57.100, 110.300 |
Unit cell angles | 90.00, 94.59, 90.00 |
Refinement procedure
Resolution | 54.973 - 2.090 |
R-factor | 0.1989 |
Rwork | 0.196 |
R-free | 0.25130 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ir1 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.041 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 65.160 | 2.200 |
High resolution limit [Å] | 2.090 | 2.090 |
Rmerge | 0.069 | 0.578 |
Number of reflections | 63709 | 9296 |
<I/σ(I)> | 11.9 | 2.6 |
Completeness [%] | 100.0 | 100 |
Redundancy | 4.4 | 4.4 |
CC(1/2) | 0.998 | 0.832 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.2 | 298 | 15% MPD, pH 5.2, VAPOR DIFFUSION, HANGING DROP, temperature 298K |