5YR0
Structure of Beclin1-UVRAG coiled coil domain complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2012-03-30 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 45.112, 45.112, 161.524 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.180 - 1.900 |
R-factor | 0.1707 |
Rwork | 0.169 |
R-free | 0.19455 |
Structure solution method | SIRAS |
RMSD bond length | 0.013 |
RMSD bond angle | 1.527 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | REFMAC (5.8.0222) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.070 | 0.165 |
Number of reflections | 8323 | |
<I/σ(I)> | 41.7 | 22.6 |
Completeness [%] | 100.0 | |
Redundancy | 20 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 0.1M citric acid pH 3.5, 3.0M sodium chloride |